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Research Applications
Pulse-Height, Charge, or Energy
Spectroscopy
Download PDF (112 KB) Spectroscopy systems for ORTEC
instrumentation produce pulse height distributions of gamma ray or alpha
energies. MAESTRO-32 (model A65-B32) is the
software included with most spectroscopy systems and includes a control
program for ORTEC hardware commonly referenced as the UMCBI. The UMCBI
provides all the drivers for the various hardware MAESTRO-32 supports.
MAESTRO-32 is an emulation software package that provides a histogram
display for pulse heights as well as utilizing the PC for display and
control functions that would normally be done in older stand alone
multi-channel pulse height analyzers. Functions in MAESTRO-32 are
typically designed for germanium detector spectra and functions like
“peak search” are looking for narrow peaks found with a germanium
detector not the broad peaks found with a sodium iodide [NaI(Tl)]
detector. Software packages for qualitative and quantitative analysis of
gamma rays are available for both germanium, sodium iodide, and alpha
spectra. Specialized application software packages are also available. Processing pulse height
information can be recorded in three ways. One method is where the
output of an analog shaping amplifier feeds into an ADC. A second method
is by using a DSP instead of an analog shaping amplifier. The detector
preamplifier output is sampled, digitized, and filtered. Then the
digitized information is displayed as a histogram. The third way is to
list each pulse height event sequentially (List Mode). List mode
requires the use of our software toolkit (Model A11-B32) to write a
program for List Mode operation. Example programs are provided in the
manuals of instruments that have list mode capability.
Detectors High-Purity Germanium
Detectors (HPGe)
Germanium detectors are
extremely large reverse biased diodes which include charge sensitive
preamplifiers that convert the charge deposited by interacting gamma
radiation into a voltage pulse which is typically filtered and amplified
for display in a pulse height histogram to exhibit the energy spectrum
of the gamma-rays collected. Germanium detectors are well known for
their superior resolution. A typical NaI detector would have on the
order of 7% resolution while an HPGe detector would have less than
0.13%. A full line of HPGe detectors is available from ORTEC including
planar and coaxial configurations. HPGe detectors need to be cooled to
near liquid nitrogen temperatures to operate. HPGe detectors far exceed
any other detector type for gamma-ray resolution. HPGe technology has
grown extensively over the past ten years. Today both laboratory and
field units are available with full analysis capability with either
liquid nitrogen or with refrigeration cooling systems.
Thallium Activated Sodium
Iodide [NaI(Tl)] Detectors
NaI(Tl) detectors incorporate a NaI(Tl) crystal mounted on a
photomultiplier tube (PMT). The NaI(Tl) crystal emits a flash of light
proportional to the energy of the gamma ray that interacts with the
crystal. The PMT detects this light and amplifies the detected light to
yield a proportional quantity of charge. This charge is converted into a
voltage pulse by a charge sensitive preamplifier. The pulse can be
discriminated by a window type (upper and lower level) Single Channel
Analyzer (SCA) and then counted, or these pulses can be displayed as a
histogram of pulse heights representing a spectrum of energy. Other Scintillator detectors are
available today such as BGO, CsI, Fast Plastic, etc. Halide detectors
have resolutions about twice as good as NaI detectors (around 3%) which
make this an attractive detector for some applications. It is important
to note that HPGe detectors still have more than 20 times better
resolution than the halides can provide. Alpha Detectors
Alpha detectors are
charged-particle silicon crystal diodes that come in various active
diameters. There are two types of detectors for alphas. The Ultra series
detectors have an ion-implanted front contact that gives a very thin
(~500 Angstrom silicon equivalence) front contact and these have
passivated leakage surfaces. These detectors are available as low
background (designated as “AS”) detectors that will fit into ORTEC
vacuum chambers. Ultra series detectors require positive bias voltage. The “ruggedized” or “R” series
detectors are made with metal evaporated contacts and have a contact
thickness on the order of ~2300 Angstroms silicon equivalence. These
detectors have epoxy covered leakage surfaces. These detectors are
available as low background (designated as “SNA”) detectors that will
fit into ORTEC vacuum chambers. R-series detectors require negative bias
voltage.
Processing Electronics Preamplifiers
HPGe detectors come with a
charge-sensitive preamplifier that integrates the charge from the
gamma-ray interaction in the detector crystal onto a capacitor in the
feedback circuit. Either a parallel resistor or a reset switch
(transistor or LED diode switch) discharges the capacitor.
NaI (Tl) detectors use a
charge-sensitive preamplifier that is stand-alone or incorporated into
the PMT base. Alpha detectors also use a
charge-sensitive preamplifier that is stand-alone or incorporated into
the alpha system.
Analog Shaping Amplifiers
Shaping amplifiers have a
selectable shaping time, t. (2.2 X t = risetime) which shapes the detector pulses for best resolution
or throughput, a pole zero circuit that allows the pulse to return to
base line long before the actual preamplifier charge pulse does, and a
base line restorer circuit to insure a consistent reference for the
pulse heights. Some shaping amplifiers incorporate logic to account for
preamplifier reset time, pulse processing time, and pile-up rejection
circuits to correct for dead times that the amplifier processing
produces. See the Amplifier section for more information. Multi-Channel Analyzers
Multi-Channel Analyzers take
their input from an analog amplifier and digitize the incoming pulse
heights placing the accumulated data into memory and displaying this
pulse height distribution in a historgram. The histogram X-axis is the
pulse height and the Y-axis is the number of counts. Today’s Multi-Channel Analyzers typically consist or a
Multi-Channel Buffer (MCB) which has an Analog-to-Digital Converter
(ADC) and a histogramming memory that can be interfaced to a PC for
display. Software (MAESTRO-32 model A65-B32)
is required to run the MCB units using the computer to make a complete
Multi-Channel Analyzer. The interface to the PC can be either by
thinwire ethernet, parallel printer port, dual port memory, or USB. The
number of channels in the ADC can determine the digital resolution which
should be chosen to suit the detector type and energy range. Signal
processing does take time and the time. The time the system is available
to receive a signal is considered “Live Time” while all the time
consumed with signal processing is “Dead Time”. MCA systems can receive
logic signals to determine this “Dead Time” in order to insure any
quantitative data is correct. DSP Units
Digital Signal Processor (DSP)
units replace the functions of the analog shaping amplifier and the MCB.
These DSP units also use MAESTRO-32 software (included with all
DSP models). DSP units typically receive a signal with a specific shape
from the preamplifier. This signal is sampled and the resulting digital
number is processed to provide a much larger range of shaping parameters
than an analog amplifier can provide. The functions of gain, baseline
restorer, pole zero, and dead time logic functions are still performed
in the DSP. Since the data is already digitized an ADC is not required.
A histogram is typically made for display on the PC. The DSP units
interface with a PC either with a dual port interface, a thinwire
ethernet interface or a USB interface (see the individual data sheets
for details).
Examples
Figures 1 through
8 show systems
for pulse-height spectrometry with a variety of detector types. The
following types are included:
Microchannel plate detector (Fig
1).
Microchannel plate photomultiplier tube (Fig. 1).
NaI(Tl) scintillation detector (Fig. 2).
Conventional photomultiplier tube (Fig. 3).
Proportional counter (Fig. 4).
Silicon charged-particle detector (Fig. 5).
Si(Li) detector (Fig. 6, 7 and 8).
Ge detector (Figs. 6, 7, and 8). If nuclear or x-ray radiation is
being detected, the pulse-height is usually calibrated in terms of the
energy of the radiation. Hence the term “energy spectroscopy” is used.
For other types of signal sources, the pulse height simply represents
the charge deposited in the detector by the event. Consequently, the
measurement process can be considered to be either “charge” or
“pulse-height” spectrometry. In Figures 1, and 3 through 7, a
preamplifier integrates the charge deposited in the detector, an
amplifier shapes the pulses for pulse-height measurement, and a
multichannel buffer (ADC plus memory) sorts the pulse heights into a
spectrum (histogram of energy versus counts). Figure 2 uses an
integrated package complete with preamplifier, high voltage supply, and
a digital signal processor all powered by the USB interface to the PC. In Figure 4, the low-noise 142PC
Preamplifier has about a factor of 6 higher sensitivity than the
standard 142IH Preamplifier. This higher sensitivity allows operation of
the proportional counter at a lower gas gain. The benefit is less
dependance of the gas gain on counting rate in the proportional counter.
As a result, the proportional counter can be operated at higher counting
rates before peak shifting occurs in the recorded energy spectrum. In Figure 6, connection
of the BUSY and PUR signals between the amplifier and MCB is essential
for achieving accurate dead time correction with the Gedcke-Hale
Live-Time Clock in the MCB.
Figures 2, 7 and 8 show the use of
an integrated electronics package for x-ray or gamma-ray spectrometry.
In this case the preamplifier output is sampled and our digital systems
provide digital signal processing for improved performance.

Figure 1.
Pulse-Height (Charge) Spectroscopy with a Microchannel Plate (µCP)
Detector, or a Microchannel Plate Photomultiplier Tube (µCP PMT).

Figure 2.
Pulse-Height (Energy) Spectroscopy with a NaI(Tl) Scintillation
Detector.

Figure 3.
Pulse-Height (Charge) Spectroscopy with a Photomultiplier Tube.

Figure 4.
Pulse-Height (Energy) Spectroscopy with a Proportional Counter.

Figure 5.
Pulse-Height (Energy) Spectrometry with a Si Charged-Particle Detector,
Including Derivation of an Optional Timing Signal.

Figure 6.
Pulse-Height (Energy) Spectroscopy with a Ge Detector for Gamma Rays, or
a Si(Li) Detector for X Rays.

Figure 7.
Pulse-Height (Energy) Spectroscopy with a Ge Detector for Gamma Rays, or
a Si(Li) Detector for X Rays, Using Digital Signal Processing (DSP).

Figure 8.
Pulse-Height (Energy) Spectroscopy with a Ge
Detector for Gamma Rays, or a Si(Li) Detector for X Rays, Using Digital
Signal Processing (DSP).
*DSPec jr 2.0, DSPec jr, or DigiDART
may also be used. |